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中药石膏X射线衍射分析及指纹图谱的确定 被引量:11

Analysis of Gypsum by X - ray Diffraction and Determination of Finger Print
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摘要 目的:考察X射线衍射分析在中药石膏质量检测与鉴别中的应用价值。方法:应用X射线衍射法对中药石膏进行定性分析,并对不同产地的10批纤维状石膏与化学试剂硫酸钙及非纤维状石膏进行分析。结果:石膏X射线衍射图谱具有很好的专属性,与其它含钙矿物药、化学试剂硫酸钙、非纤维状石膏区别明显,10批纤维状生石膏指纹图谱相似度均达到95%以上。结论:石膏的X射线衍射指纹图谱可全面地、客观地反映出石膏的内在质量特征。X射线衍射分析方法专属性强,准确可靠,可作为石膏质量检测与鉴别的手段, Objective: To investigate the applied value of qualitative determination and distinguish for gypsum with X-ray diffraction. Methods: With X-ray diffraction for qualitative analysis of Gypsum, the fibriform and non-fibroid gypsum and chemical reagent calcium sulfate in 10 group and from different producing areas were analyzied. Results: The X-ray diffraction atlas of gypsum was exclusive and different remarkably from the other mineral medicines including calcium, non -fibroid gypsum and chemical reagent calcium sulfate. All the finger prints of the fibriform gypsum from each group were similar and the comparability was over 95%. Conclusion:The X-ray diffraction can express objectively the interior quality of the gypsum, which is specificity, accuracy and reliability and can be used for the determination of Gypsum.
出处 《世界中西医结合杂志》 2006年第2期91-93,共3页 World Journal of Integrated Traditional and Western Medicine
基金 国家"十五"重大科技专项"创新药物和中药现代化"课题 NO:2111BA701A55-32
关键词 中药石膏 X射线衍射 指纹图谱 gypsum X-ray diffraction fingerprint
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  • 1吕扬,药学学报,1993年,28卷,442页
  • 2张汉明,中草药,1992年,23卷,84页
  • 3唐长馥,中国医药学报,1988年,3卷,27页
  • 4张绶庆,非金属矿物工学,1962年

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