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Total synthesis of endothelin 1 by microwave-assisted solid phase method 被引量:1

Total synthesis of endothelin 1 by microwave-assisted solid phase method
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摘要 A microwave-assisted solid phase synthesis for endothelin 1 is presented.Reduced endothelin 1 was synthesized efficiently on Wang resin under microwave irradiation using Fmoc/tBu orthogonal protection strategy.The whole peptide was cleaved from the resin and two disulphide bridges were formed under air oxidation at room temperature.The purity and efficiency of synthesizing the peptide is much higher than other methods used before.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2010年第4期388-390,共3页 中国化学快报(英文版)
基金 supported by the key project of Chinese Ministry of Education(No.109086)
关键词 Endothelin 1 Microwave irradiation Solid phase Disulphide bridge Endothelin 1 Microwave irradiation Solid phase Disulphide bridge
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