摘要
目的 研究决明子中总蒽醌的提取工艺。 方法 采用正交试验法进行优选 ,紫外分光光度法测定总蒽醌含量。 结果 乙醇浓度对提取有极显著性影响。 结论 最佳提取工艺为决明子粗粉 ,用 90 %乙醇回流提取 2次 ,每次 6倍量溶剂 ,提取 1h。
OBJECTIVE To study the extraction process for the total anthraguinones in Semen cassiae.METHODS The optimum extraction process was selected with the orthogonal design.The content of total anthraquinones was determined by uv-Spectrophotometry.RESULTS The alcohol concentration was remarkable factor in the test.CONCLUSION The optimum extraction process is as follows:adding 6 time amount of90 % alcohol into materials and refluxing and extracting for2 times,1 h every time.
出处
《海峡药学》
2004年第4期14-16,共3页
Strait Pharmaceutical Journal
关键词
决明子
正交试验
总蕙醌
提取工艺
紫外分光光度法
Sem en cassiae
Orthogonal Design
total anthraquinones
extraction process
uv- Spectrophotometry