摘要
研究了用烯丙基氯与N,N二甲基苯胺为原料合成二甲基烯丙基苯基氯化铵的方法,测定了不同温度、原料配比、反应时间和不同溶剂条件下目的物的产率,并对产物的结构进行了表征。
In this paper,dimethylallylphenylammonium chloride was made from allyl chloride and N,N dimethylaniline.The yields at various temperatures,reaction mixture composition,reaction time and different solvents were studied.The yields were determined by NaBPh 4 gravimetric analysis.The structure of dimethylallylphenylammonium chloride was characterized by IR and 1HNMR .
出处
《化学试剂》
CAS
CSCD
北大核心
2004年第4期195-196,200,共3页
Chemical Reagents