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X-ray Structure of Bis(salicylidene)-p-diaminobenzene

X-ray Structure of Bis(salicylidene)-p-diaminobenzene
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摘要 The crystal and molecular structures of Schiff base bis(salicylidene)-p-diaminobenzene were determined by X-ray crystallography. It crystallized in a monoclinic system with space group P2(1)/c, lattice parameters a=1.4649(3) nm, b=0.45770(9) nm, c=1.2241(2) nm, α=γ=90.00°, β=112.07(3)°, V=(0.7606(3) nm^3,) and Z=4. The crystal structure of the title compound is composed of discrete monomeric molecule of ((C_6H_4)(NCC_6H_4OH)_2) which is planar. The intermolecular hydrogen bonds make the compound steady. The crystal and molecular structures of Schiff base bis(salicylidene)-p-diaminobenzene were determined by X-ray crystallography. It crystallized in a monoclinic system with space group P2(1)/c, lattice parameters a=1.4649(3) nm, b=0.45770(9) nm, c=1.2241(2) nm, α=γ=90.00°, β=112.07(3)°, V=(0.7606(3) nm^3,) and Z=4. The crystal structure of the title compound is composed of discrete monomeric molecule of ((C_6H_4)(NCC_6H_4OH)_2) which is planar. The intermolecular hydrogen bonds make the compound steady.
出处 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 2004年第5期562-564,共3页 高等学校化学研究(英文版)
基金 Supported by the National Natural Science Foundation of China(No.2 0 2 75 0 2 0 ) the Natural Science Foundation ofShandong Province(No.Z2 0 0 2 B0 2 ) and the Outstanding Adult- young Scientific Research Encouraging Foundation of Shan-dong Provinc
关键词 Schiff base Salicylidene Hydrogen bond Schiff base, Salicylidene, Hydrogen bond
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