摘要
报道了由ＰＯＣｌ＿３、乙二醇和环氧乙烷反应合成阻燃剂Ｔｈｅｒｍｏｌｉｎ１０１的新合成路线。研究了影响反应的因素，反应收率可达到９０％。经红外光谱、核磁共振和元素分析测定了产品的化学结构，并做了在聚氨酯软泡中的应用试验，和阻燃涂层试验，结果显示Ｔｈｅｒｍｏｌｉｎ１０１是一种较好的新型阻燃剂。
In this paper a new synthesis method for flame retardant Thermolin 101 from POCl_3,glycol and ethylene oxide was reported. The factors which influence the reaction werestudied.The yield reaehed 90%. The chemical structure of the product was exalnined byusing IR, NMR and elemental analysis.Application test in soft polyurethane foam and flameretardant coating test were made. It shows Thermolin 101 is a new good flame retardant.
出处
《石油化工》
EI
CAS
CSCD
北大核心
1994年第8期527-531,共5页
Petrochemical Technology
关键词
阻燃剂
环氧乙烷
合成
乙二醇
flame retardant,Thermolin 101,ethylene oxide,synthesis method,soft poly-urethane foam, flame retardant coating test
