摘要
以苯甲醛和环己酮为原料,在碱性条件下,采用相转移催化法,利用微波技术制备了α,α′-二亚苄基环己酮,并用FTIR、1HNMR和MS表征了该化合物的结构。该法具有操作简单、产率高、污染少等优点。
α,α′-Bis(benzylidene) cyclohexanone was successfully prepared from phenyl formaldehyde and cyclohexanone at base conditions by the means of phase transfer catalysis method and microwave technology. The compound was characterized by FTIR、 1 HNMR and MS. This method had some advantages of simple operation, high yield and little contamination.
出处
《化学与生物工程》
CAS
2005年第6期21-22,共2页
Chemistry & Bioengineering
关键词
α
α'-二亚苄基环己酮
微波
合成
α,α′-bis(benzylidene) cyclohexanone
microwave
synthesis
