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柱色谱分离提纯2-氯-5-三氯甲基吡啶的研究 被引量:2

Study of Using Pillar Chromatography to Separate and Purify 2-chloro-5-Trichloromethylpyridine
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摘要 2-氯-5-三氯甲基吡啶是重要的医药和农药中间体.研究用柱色谱方法对3-甲基吡啶光氯化产物进行分离和提纯,制备高纯度的2-氯-5-三氯甲基吡啶.通过毛细管气相色谱检测纯度,结果表明产物纯度为90%以上. chloro-5-trichloromethylpyridine is an important middle product of medicine and agricultural chemical. This article studies using pillar chromatography to separate and purify those products about lighting and chlorining 3-methylpyridine. We examine purity through capillary column gas chromatography.The result indicats that purity of the product is over 90%.
出处 《湘南学院学报》 2005年第2期54-56,共3页 Journal of Xiangnan University
关键词 2-氯-5-三氯甲基吡啶 3-甲基吡啶 柱色谱 分离提纯工艺 methylpyridine 2-chloro-5-trichloromethylpyridine chromatography/mass spectrometry
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