摘要
合成了高氯酸钕与咪唑、DLα丙氨酸的配合物晶体.用傅立叶变换红外光谱(FTIR)、元素分析和学分析确定其组成为[Nd(C3H7NO2)2(C3H4N2)(H2O)](ClO4)3.用差示扫描量热法(DSC)对配合物的热稳定进行了研究,发现配合物有较高的热稳定性.
The crystal of complex of rare-earth neodymium perchlorate with imidazole and DL-α-Alanine was synthesized and characterized. The components of complex was determined to be [Nd(C3H7NO2)2(C3H4N2)(H2O)](ClO4)3 by the FT-IR, dement analysis and chemical analysis. The thermal stability of complex was determined by differential scanning calorimetry (DSC), The result showed the complex have higher thermal stability.
出处
《中央民族大学学报(自然科学版)》
2005年第3期261-263,共3页
Journal of Minzu University of China(Natural Sciences Edition)
基金
湖北民族学院2003年重点科研项目.
关键词
稀土配合物
合成
差示扫描量热法(DSC)
热稳定性
rare-earth complex
synthesis
differential scanning calorimetry(DSC)
thermal stability