摘要
目的:建立乌梅人丹的质量标准;方法:对制剂中乌梅用薄层色谱法进行定性鉴别,同时采用气相色谱法测定制剂中薄荷脑含量以及采用高效液相色谱法测定制剂中甘草酸铵的含量。结果:平均回收率分别为103.5、100.3,RSD分别为0.76(n=6)和1.03(n=6)。薄层图谱斑点清晰,空白无干扰。结论:方法简便、准确、重现性好,可有效控制该制剂的质量。
AIM ： To establish the quality standard of Wumeirendan （ Fructus Mume, Radix et Rhizoma Glycyrrhizae, Mentholm, etc. ） METHODS： Fructus Mume was identified by TLC. Menthol was determined by GC, Ammonium glycyrrhiziate was determined by HPLC. RESULTS： The average recoveries were 103.5% and 100. 3% , RSD were 0.76% and 1.03%. The TLC sports developed were fairly clear, and the blank test showed no interference. CONCLUSION：The method developed is simple and accurate with good reproducibility, and the method can be used for quality control of Wumeirendan.
出处
《中成药》
CAS
CSCD
北大核心
2005年第8期896-899,共4页
Chinese Traditional Patent Medicine
