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马铃薯淀粉羧甲基化过程的优化 被引量:3

Optimization of the carboxymethyl process of potato starch
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摘要 羧甲基马铃薯淀粉被广泛应用于工业部门。本文将水分、温度、反应时间、理论取代度(DSt)、淀粉负荷以及氢氧化钠对一氯乙酸钠的摩尔比(nNaOH/nSMCA)作为马铃薯淀粉羧甲基化过程的影响因素,利用响应曲面法中的Box-Behnken设计法对过程进行了优化,并用Matlab中的二次响应曲面函数对结果进行了分析,最终得到了马铃薯羧甲基化过程的最佳反应条件,制备所得羧甲基马铃薯淀粉产物取代度高达DS=1.0602。 The carboxymethyl potato starch (CMS) is used in industries extensively. The effective factors, such as fraction of water, temperature, reaction time, theoretical degree of substitution, starch fraction and molar ratio of sodium hydroxide to sodium monochloro acetate, were optimized through Box-Behnken design, which belongs to the surface response methodology. The results was analyzed quadratic response surface function of Matlab, and the optimized conditions of carboxymethylation was concluded finally. The DS about 1. 0602 of carboxymethyl starch was produced in the optimized conditions.
出处 《计算机与应用化学》 CAS CSCD 北大核心 2005年第8期651-654,共4页 Computers and Applied Chemistry
关键词 羧甲基马铃薯淀粉 取代度 Box—Behnken设计法 carboxymethyl potato starch, degree of substitution, Box-Behnken design
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  • 1武宗文.羧甲基淀粉生产应用现状及发展方向[J].郑州粮食学院学报,1998,19(2):82-86. 被引量:27
  • 2Yao J, Chen WR and Robbert Manurung M et al. Exploratory Studies on the Carboxymethylation of Cassava Starch in Water-miscible Organic Media. Starch/Starke, 2004, 56:100- 107.
  • 3Tijsen CJ, Kolk HJ, Stamhuis EJ, Beenackers AACM. An experimental study on the Carboxymethylation of granular potato starch in non-aqueous media. Carbohydr, Polym, 2001, 45:219 - 226.
  • 4Bhattacharyya D, Singhal RS and Kulkarni PR:A comparative account of conditions for synthesis of sodium carboxymethyl starch from corn and amaranth starch. Carbohydr Polym, 1995, 27:247 - 253.
  • 5杨德全,王升文,刘启瑞,周海兵,刘玉婷.影响淀粉渣羧甲基化产物取代度的因素研究[J].延安大学学报(自然科学版),1996,15(3):49-51. 被引量:4
  • 6DouglasC Montgomery 汪仁官 陈荣超译.实验设计与分析[M].北京:中国统计出版社,.589-623.
  • 7Patrick D, Shaw Stewart and Peter FM Baldock. Practical experimental design techniques for automatic and manual protein crystallization. Journal of Crystal Growth, 1999, 196:665 -673.
  • 8Anees A, Karnachi and Mansoor A Khan. Box-behnken design for the optimization of formulation variables of indomethacin coprecipitates with polymer mixtures. International Journal of Pharmaceutics, 1996, 131:9 - 17.
  • 9Heinze T, Erler U, Nehls I, Klemm D. Determination of the substituent pattern of heterogeneously and homogeneously synthesized carboxymethyl cellulose by using high-performance liquid chromatography, Angew Macromol Chem, 1994, 215, 93 - 106.
  • 10Qiu H and He L. Synthesis and properties study of carboxymethyl cassava starch. Polym Adv Technol, 1999, 10:468 -472.

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