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树脂热解炭制备SiC纳米微粉 被引量:2

Synthesis of Nanometer SiC Powder From Resin Char
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摘要 用自制的酚醛树脂热解炭作炭源,用SiO2纳米微粉作硅源,根据碳热还原原理,利用常规加热和微波加热两种方式,分别制备了SiC纳米微粉.X射线衍射、分析电镜检测结果表明:制备工艺和条件对SiC纳米微粉的性质有较大的影响. A method for formation of nanometer powder from resin char was described. Namometer SiC powder was syothesed by the reduction of SiO2 with C in an atmosphere of nitrogen. Nanometer SiO2 powder, phenolformaldehyde resin and resin char were used as starting materials. The properties of the powder were determined by means of XRD, TEM, and so on. The results show that technique and condition for preparing samples have obvious effects on the powder characteristics.
出处 《无机材料学报》 SCIE EI CAS CSCD 北大核心 1996年第2期361-364,共4页 Journal of Inorganic Materials
基金 国家高技术新材料领域专家委员资助
关键词 酚醛树脂 热解炭 纳米微粉 碳化硅陶瓷 制备 phenolformaldehyde resin,char,SiC,nanometer powder
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参考文献2

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同被引文献30

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  • 3戴长虹,张显鹏,张劲松,杨永进,曹丽华,夏非.AlN纳米微粉的微波合成[J].物理化学学报,1996,12(11):1049-1051. 被引量:8
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