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GC测定感冒康喷雾剂中桉油精、樟脑、薄荷脑和龙脑的含量 被引量:11

Determination of eucalyptol, camphor, menthol and borneol in Ganmaokang Spray by GC
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摘要 目的:建立中药复方制剂中桉油精、樟脑、薄荷脑和龙脑含量测定的方法。方法:采用毛细管气相色谱法,弹性石英毛细管柱(30m×0.53mm×1.2μm)EC—WAX;萘为内标。结果:桉油精、樟脑、薄荷脑和龙脑线性范围分别为0.38448~0.89712mg/mL,0.2406—0.5614mg/mL。0.36756—0.8576mg/mL,0.1356—0.3164mg/mL;平均加样回收率分别为98.4%,98.2%,98.5%,98.2%(n=5)。结论:该方法快速、方便,分离度好,其他成分无干扰,适用于复方制剂中4种成分的同时测定。 AIM: To establish a method of determining eucalyptol, camphor, menthol and borneol in Ganmaokang Spray. METHODS : GC was conducted on a EC-WAX column (30 m × 0.53 mm × 1.2 μm) and naphthalene was adopted as internal standard. RESULTS: Eucalyptol, camphor, menthol and borneol respectively showed a good linear relationship in the following ranges of concentration: 0. 384 48-0. 987 12 mg/mL, 0. 240 6 0. 561 4 mg/mL,0. 367 56-0.857 6 mg/mL and 0. 135 6-0.316 4 mg/mL. The average recoveries were obtained as 98.4%, 98.2% , 98.5% and 98.2% ( n = 5). CONCLUSION: The method is simple, sensitive, accurate and suitable for the determination of four constituents in Ganmaokang Spray.
作者 苏健俊 丁野
出处 《中成药》 CAS CSCD 北大核心 2006年第1期39-41,共3页 Chinese Traditional Patent Medicine
关键词 感冒康喷雾剂 桉油精 樟脑 薄荷脑 龙脑 Ganmaokang Spray eucalyptol camphor menthol borneol
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