摘要
用高效液相色谱法测定麻杏止痰丸中盐酸麻黄碱的含量,色谱柱:Hypersil ODS 2,流动相:甲醇-水(1:1);检测波长:254nm;流速:1.0ml·min^-1。线性范围为0.012~0.060μg,r=0.9996;平均回收率为97.1%,RSD为1.09%。本法简便,灵敏,准确。
A HPLC method was established for the determination of ephedrine hydrochloridt in Maxingzhitan Pills. A Hypersil ODS 2 column was used with the mobile phase of methanol - water (1 : 1) and the flow rate 1.0ml · min^-1. The detection wavelength was 254nm. The good linear range was within 12~60μg (r=0. 9996), average recovery was 97.1% and RSD was 1.09%, The method was simple, sensitive and accurate.
出处
《中国药事》
CAS
2006年第2期108-110,共3页
Chinese Pharmaceutical Affairs