期刊文献+

1-苯甲酰基-3-芳基硫脲与肼的成环反应研究

Study on the cyclic reaction between 1-benzoyl-3-arylthiourea and hydrazine hydrate
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摘要 1-苯甲酰基-3-芳基硫脲和水合肼反应生成了3-苯基-5-芳胺基-4H-1,2,4-三氮唑,产物结构经红外光谱、核磁共振光谱和高分辨质谱表征. 3 - Phenyl - 5 - arylamido - 4H - 1,2,4 - triazole was prepared by the reaction of hydrazine hydrate with 1 - benzoyl - 3 - arylthiourea, its structure was characterized by IR, NMR and HRMS spectra.
出处 《苏州大学学报(自然科学版)》 CAS 2006年第1期78-79,88,共3页 Journal of Soochow University(Natural Science Edition)
基金 江苏省有机合成重点实验室资助项目(JSK016)
关键词 1-苯甲酰基-3-芳基硫脲 三氮唑 合成 1 - benzoyl - 3 - arylthiourea triazole synthesis
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参考文献3

  • 1ZENG R S, ZOU J P, ZHI S J,et al . Novel synthesis of 1-aroyl-3-aryl-4-substituted imidazole-2 thiones[J]. Org Lett, 2003, (10) : 1657 - 1659.
  • 2吴君臣,安礼涛,穆学军,邹建平.1,3-二溴丙酮与苯基硫脲的反应研究[J].苏州大学学报(自然科学版),2005,21(2):68-69. 被引量:4
  • 3KATRITZKY A R, CAI X H, ROGOVOY B V. Solid phase synthesis and application of trisubstituted thioureas[J]. J Comb Chem, 2003, (5) ,392 - 399.

二级参考文献4

  • 1MARCANTONIO K M,CHEN C Y.Apractical preparation of 5-(ketoaryl)thiazoles[J].Tetrahedron Letters,2002,43:8845-8848.
  • 2TAYLOR R E,HALEY J D.Towards the synthesis of epothilone A:enantioselective preparation of the thiazole sidechain and macrocyclic ring closure[J].Tetrahedron Letters,1997,38:2061-2064.
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  • 4MENGER F M,PERSICHETTIR R A.Two new amphiphilic catalysts for ester hydrolysis[J].J Org Chem,1987,52:3451-3452.

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