摘要
本文采用气相色谱法，分离测定了鸦胆子油乳制剂中油酸的含量。以２０％丁二酸二乙二醇聚酯（ＤｉｅｔｈｙｌｅｎｅＧｌｙｃｏｌＳｕｃｃｉｎａｔｅ，简称ＤＥＧＳ）为固定相，酸洗铬姆沙伯Ｗ（ＣｈｒｏｍｏｓｏｒｂＷ－ＡＷ）６０～８０目为担体，柱温１７５℃，苯甲酸苯酯为内标。线性范围为０．３２～１．６０μｇ，相关系数为０．９９８４，平均回收率为９９．８％（口服乳）和１００．１％（乳冲剂）。
The method of quantitative determination of oleic acid in Brucea javanica oil by gas chromatography is established. The determination condition were: liquid phase, 20% DEGS; support,chromosorb W-AW (60～80 mesh); column temperature, 175℃, injection port temperature,250℃; FID detector; phenylbenzoate as the internal standard. The standard curve is linear within the range of 0. 32～1. 60μg of Brucea javanica oil and correlation coefficient is 0. 9984.
出处
《药物分析杂志》
CAS
CSCD
北大核心
1996年第2期98-100,共3页
Chinese Journal of Pharmaceutical Analysis
