摘要
建立HPLC法测定强生胶囊中橙皮苷含量的方法。采用phenomenex C18色谱柱，乙腈-0．2％磷酸（20：80）为流动相；流速1.0ml·min^-1；检测波长284nm。橙皮苷在0．27～2．16μg范围之间线性关系良好（r=0.9999），平均回收率98．3％，RSD2．54％。本方法简便，重现性好，可有效控制制剂质量。
A HPLC method was established for determination of hesperidin in Qiangsheng Capsules. A phenomenex C18 column was used with acetonitrile-0.2% phosphoric acid （20 ： 80） as mobile phase, and the detecting wavelength was 284nm. There was a good linear relationship （r=0. 9999） when the content of hesperidin was 0. 27-2. 16μg. The average recovery was 98. 3% and RSD was 2. 54%. The method was simple and reproductive. It could be used for quality control of the preparation.
出处
《中国药事》
CAS
2006年第6期358-359,共2页
Chinese Pharmaceutical Affairs
