摘要
本文详细研究了氰化物蒸馏条件及其稳定性问题，建立了一个冷原子荧光法间接测定水中氰化物的方法，并用于海水及氰化液中痕量ＣＮ－的测定，结果令人满意。ＣＮ－检出限为０．０２μｇ／ｍＬ，回收率９５％～９８％，变异系数７．３％～８．９％。
A cold atomic fluorescence method for the indirect determination of cyanides is described.The distillation and stabilization conditions have been studied carefully.This method has high sensitivity and good reproducibility.It has been applied successfully to the determination of trace amounts of cyanides in sea water and cyanide bath liquor.The detection limit is 0.02 μg/mL.The recovery is 95%～98%,while the variation coefficient is 7.3%～8.9%.
出处
《分析测试学报》
CAS
CSCD
1996年第5期56-59,共4页
Journal of Instrumental Analysis
