摘要
以乙酸和环己醇为原料，六水合三氯化铝为催化剂催化合成了乙酸环己酯。在优化反应条件下，酯收率达78．8％。优化反应条件如下：n（乙酸）：200mmol，n（乙酸）：n（环己醇）=1．0：1．5，催化剂用量为1．5g，带水剂环己烷用量为10mL，反应温度为106．124％。实验结果表明催化剂催化性能高，反应条件温和，方法简单，收率优良。
Cyclohexyl acetate was synthesized from acetic acid and cyclohexanol catalyzed by aluminum chloride hexahydrate. Optimum conditions of estefification were determined with yield of 78.8 %. They were as follows ： molar ratio of cyclohexanol to acetic acid is 1.0：1.5; amount of catalyst is 1.5 g; mount of cyclohexane is 10 mL and temperature of reaction is 106 - 124℃. The experiment indicated high catalytic activity, mild conditions, convenient method and excellent yield.
出处
《化工时刊》
CAS
2006年第10期33-34,共2页
Chemical Industry Times
关键词
乙酸环己酯
六水合三氯化铝
催化
合成
cycloheaxyl acetate alumimum chloride hexahydrate catalysis synthesis
