摘要
以对甲基氯化苄与二甲基烯丙基胺为原料合成了二甲基烯丙基对甲基苄基氯化铵,考查了光照、氮气保护、避光、温度、原料配比、反应时间和不同溶剂等因素对反应的影响,通过四苯硼钠的定量分析确立了最佳反应条件,并对产物的结构进行了表征.
Dimethyl allyl p-methylbenzyl ammonium chloride was synthesized from p-methylbenzyl chlo- ride and dimethyl allylamine. The factors affecting the reaction, such as temperature, reaction composition, reaction time, solvent and so on were investigated. The yields were determined by gravimetric analysis with NaBPh4. The structure of the product was characterited by IR, ^1H NMR and MS.
出处
《化学研究》
CAS
2006年第4期54-55,59,共3页
Chemical Research
关键词
阳离子单体
季铵盐
二甲基烯丙基对甲基苄基氯化铵
cationic monomer
quaternary ammonium salt
dimethyl allyl p-methylbenzyl ammonium chloride
