摘要
采用了11种实验室模拟工艺(650~750℃、1.5~873h),利用TEM、SEM、OM等考察了珠光体耐热钢12Cr1MoV高温长时间加热后成分、组织结构与性能的变化.研究表明,试验用钢在高温时效后其组织结构明显退化,固溶体内合金元素Cr、Mo、V严重贫化(其中Mo的降幅为2/3),发生晶粒长大(~70%),碳化物向晶界的聚集粗化,以及相变位错密度显著降低和位错胞尺寸变大及消散等,同时基体硬度下降30%.多层次结构综合分析表明,12Cr1MoV耐热钢高温时效中,由于组织结构的退化,引起其性能的劣化,导致材料的弱化(老化).
The variation of compositions, microstructures and properties of pearlitic heat resistant steal 12 Crl MoV after elevated temperature-long term heating, with eleven kinds of experimental simulation proces- ses(650 ~ 750℃ and 1.5 ~ 873 h) , has been examined by means of TEM, SEM and OM, etc.. It is concluded that, after high-temperature aging, the microstructure of the tested material degrades obviously, the alloy elements (Mo,Cr,V) in solid solution are diluted deeply ( variation of Mo, about 2/3 ) , its grains grow considerably( ~ 70% ) , carbides coarsen and aggregate toward grain boundaries, the density of phase transformation dislocation reduces greatly and size of dislocation cells increases then disappears progressive- ly. Meanwhile, the hardness of the tested material matix reduces(about 30% ). The analysis shows that, during high temperature aging, the material weakening of the tested heat-resistant steel 12CrMoV is contributed to its microstructure degeneration which causes its mechanical property to deteriorate.
出处
《材料科学与工艺》
EI
CAS
CSCD
北大核心
2007年第2期221-224,共4页
Materials Science and Technology
基金
甘肃省自然科学基金资助项目(ZS001-A22-046-C)
关键词
耐热钢
珠光体
时效
退化
heat resistant steel
pearlite
aging
degeneration