摘要
目的:评定以紫外分光光度法测定酚酞片含量的不确定度。方法:根据《测量不确定度评定与表示》,并参考《化学分析中不确定度的评估指南》,对酚酞片的含量测定进行测量不确定度的分析与评定。结果:扩展不确定度为1.0%,相对扩展不确定度为1.0%,含量测定结果可表示为(97.0±1.0)%。结论:严格按照操作规范,尽可能减少稀释过程影响,可有效降低引入的不确定度,保证测定结果准确。
OBJECTIVE: To evaluate the uncertainty in the determination of the content of phenolphthalein tablet by UV spectrophotometry. METHODS: The uncertainty in the determination of the content of phenolphthalein tablet was analyzed and evaluated based on"Evaluation and Expression of Uncertainty Measurement"and the"Manual of Uncertainty Evaluation in Chemical Analysis". RESULTS: Both the expanded uncertainty U95 and the relative expanded uncertainty Urel were 1.0%. The content of phenolphthalein tablet was (97.0 ± 1.0) %. CONCLUSION: The introduced uncertainty can be effectively reduced and the determination result can be ensured by strictly following the operation standards and trying to reduce the in-fluence of the dilution process.
出处
《中国药房》
CAS
CSCD
北大核心
2007年第19期1500-1501,共2页
China Pharmacy
关键词
酚酞片
紫外分光光度法
含量
不确定度
评定
Phenolphthalein tablet
UV spectrophotometry
Content
Uncertainty
Evaluation