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Macro-microscopic morphology and phase analysis of TiAl-based alloys sheet fabricated by EB-PVD method 被引量:6

Macro-microscopic morphology and phase analysis of TiAl-based alloys sheet fabricated by EB-PVD method
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摘要 TiAl-based alloys sheet with thickness of 0.3-0.4 mm as well as dimension of 150 mm×100 mm was fabricated successfully by using electron beam-physical vapor deposition(EB-PVD) method. The microscopic morphology and phase composition of specimens in various states were analyzed by atomic force microscope(AFM), scanning electron microscope(SEM) and X-ray diffractometer(XRD), respectively. The results indicate that the as-deposited TiAl-based alloys sheet has good surface quality and is composed of γ, α2 and τ phase. There is natural delamination inside the sheet, of which the microstructure is columnar crystal, and the component shows a gradient change along the normal direction of substrate. After the vacuum hot pressing treatment and subsequent homogenization treatment, the columnar crystal transforms into the coarse fully lamellar microstructure, the delamination phenomenon and τ phase disappear, α2 phase decreases obviously, and the composition tends to uniformization. TiAl-based alloys sheet with thickness of 0.3-0.4 mm as well as dimension of 150 mm×100 mm was fabricated successfully by using electron beam-physical vapor deposition(EB-PVD) method. The microscopic morphology and phase composition of specimens in various states were analyzed by atomic force microscope(AFM), scanning electron microscope(SEM) and X-ray diffractometer(XRD), respectively. The results indicate that the as-deposited TiAl-based alloys sheet has good surface quality and is composed of γ, α2 and r phase. There is natural delamination inside the sheet, of which the microstructure is columnar crystal, and the component shows a gradient change along the normal direction of substrate. After the vacuum hot pressing treatment and subsequent homogenization treatment, the columnar crystal transforms into the coarse fully lamellar microstructure, the delarnination phenomenon and τ phase disappear, α2 phase decreases obviously, and the composition tends to uniformization.
出处 《中国有色金属学会会刊:英文版》 EI CSCD 2007年第4期777-782,共6页 Transactions of Nonferrous Metals Society of China
基金 Project(90405016) supported by the National Natural Science Foundation of China
关键词 钛铝合金 电子束-物理气相沉积 微观结构 相分析 TiAl-based alloy electron beam-physical vapor deposition sheet morphology phase analysis
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