摘要
目的:制定阴洗液的质量标准。方法:采用薄层色谱法鉴别阴洗液中苦参、蛇床子、黄柏,高效液相色谱法测定蛇床子素的含量,采用phenomenx C18色谱柱(4.6mm×150mm,5μm),流动相:甲醇-0.1%磷酸溶液(70:30),流速1.0ml·min^-,柱温:40℃,检测波长:322mm。结果:薄层斑点清晰,含量测定重现好,蛇床子素在0.03804~0.192μg范围内线性关系良好,平均回收率为97.62%,RSD%=1.04%。结论:方法简便,准确,可供本品质量控制。
Objective : To establish the quality standard of Yinxi lotion. Method : The TLC method was used to identify lightyel- low sophora root, fruetus; amooreon tree hark; the HPLC method was used to determine the content of osthole. Result: The spot was clear with good reproducibility in content determination, the average recovery was 97.62% with RSD% 1.04%. Conclusion: The method is simple; accurate, can be used as quality control for this preparation.
出处
《中医药导报》
2007年第10期79-80,93,共3页
Guiding Journal of Traditional Chinese Medicine and Pharmacy