摘要
目的合成标题化合物,并进行工艺改进。方法以邻苯二甲酰亚胺为原料经次氯酸钠氧化合成目标化合物。结果收率达90%以上,产物经红外和核磁共振谱确证。结论改进的路线原子经济、环境友好,易操作。
OBJECTIVE To synthesize the tide compound and improve the process. METHODS The title compound was synthesized from phthalimide by oxidation with sodium hypochlorite. RESULTS The yield was up to 90%, the tide compound was characterized by IR and ^1 HNMR. CONCLUSION The process has many advantages from economical and environmental point of view and it is easy to handle.
出处
《中国现代应用药学》
CAS
CSCD
北大核心
2007年第6期473-474,共2页
Chinese Journal of Modern Applied Pharmacy
