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三种邻香兰素还原型席夫碱-镍(Ⅱ)配合物的合成及表征 被引量：2

Synthesis and characterization of three reduced Schiff base of o-vanillin-amino acids and their nickel(Ⅱ) complexes
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摘要 Three new reduced Schiff base derived from o-vanillin and amino acids such as alanine, leucine, and phenylalanine are prepared through condensation, reduction, and acidification. Their Ni(Ⅱ) complexes are also synthesized by the reduction of Schiff base, respectively.All new synthesized compounds are characterized by element analysis, atomic absorption spectrophotometry, and infrared spectra. Meanwhile the thermal stability and DRS UV/Vis of three complexes are also studied. Three new reduced Schiff base derived from o - vanillin and amino acids such as alanine, leucine, and phenylalanine are prepared through condensation, reduction, and acidification. Their Ni （ Ⅱ） complexes are also synthesized by the reduction of Schiff base, respectively. All new synthesized compounds are characterized by element analysis, atomic absorption speetrophotometry, and infrared spectra. Meanwhile the thermal stability and DRS UV/Vis of three complexes are also studied.
作者 孙露 赵干卿 陈敏 陆晓青 荆俊杰 谢吉民
机构地区 江苏大学化学化工学院
出处 《化学研究与应用》 CAS CSCD 北大核心 2008年第3期295-298,共4页 Chemical Research and Application
基金 江苏省高新技术项目(BG2007025)资助 江苏省社会发展项目(BS2006038)资助 镇江市社会发展项目(SH2006057)资助
关键词 邻香兰素 还原席夫碱 配合物 o - vanillin reduced Schiff base complex
分类号 O625.632 [理学—有机化学]
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化学研究与应用
2008年 第3期

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