摘要
本文介绍了合成配合物[(C3S5)2Zn](NBu4)2的三种方法—Steimecke合成法、溶剂热合成法和冰浴合成法.对三种合成方法的优缺点做了比较和分析,并对每种方法的反应条件进行了优化.
In this paper, the three synthetic methods of coordination complexes [(C3S5)2Zn](NBu4)2 - Steimeeke Method, lee Bath Method and Solvent Thermal Synthesis Method - have been introduced. It conducts a comparison of the three methods, and meanwhile, the advantages and drawbacks of the three methods were analyzed and compared, and put forword fitting condition of each method.
出处
《内蒙古民族大学学报(自然科学版)》
2008年第1期34-36,共3页
Journal of Inner Mongolia Minzu University:Natural Sciences
基金
内蒙古民族大学自然科学基金项目(MDX2007038)
关键词
合成
Steimecke法
溶剂热法
冰浴法
Synthsize
Steimeeke method
lee bath method
Solvent thermal synthesis method