摘要
目的建立测定排氚片中黄芪甲苷含量方法。方法采用薄层扫描法测定黄芪甲苷含量，硅胶G薄层预制板，氯仿-甲醇-水（13：6：2）10℃以下放置过夜的下层溶液为展开剂，测定波长530nm，参比波长700nm。结果黄芪甲苷点样量在0．20～0．701μg之间和吸收度积分值呈良好的线性关系，平均回收率为96．74％，RSD为2．02％。结论薄层扫描法便捷、灵敏、准确，可作为排氚片的质量控制方法。
Aim To develop a method for determining the content of astragaloside IV in paichuan tablets by TLC - scanning. Methods Silica G was used as the solid phase and developed with Chloroform-Methanol-Water （ 13： 6：2）; λS = 530nm, λR = 700nm. Results A good linearity of astragaloside IV was obtained within the range of 0.20-0. 70μg. The average recovery was 96.74% and RSD was 2.02%. Conclusion The method was simple, accurate, reliable and can be used as the quality control of this preparation.
出处
《解放军药学学报》
CAS
2008年第3期258-260,共3页
Pharmaceutical Journal of Chinese People's Liberation Army
基金
全军十一五重点课题
No.200603004
