摘要
C60与α-氨基酸和醛酮反应生成N-未取代的C60吡咯烷衍生物。本文给出了用柱层析法分离纯化产物的一般原理和过程，总结了用FD－MS，FT－IR，UV－Vis，1H－NMR和13C－NMR表征产物结构时所给出的共同特征。
N-unsubstituted [60] fulleropyrrolidine derivatives, which are obtained from the reaction of C60 with a-aminoacid and aldehyde or ketone, can be isolated by flash column chromatography on silica gel. Their structures can be characterized by FD-MS, FT-IR,UVVis. 1H-NMR and13C-NMR.
基金
江西省自然科学基金
中科院开放基金
关键词
吡咯烷衍生物
碳60
提纯
结构表征
[60]Fulleropyrrolidine derivative, Purification, Characterization
