摘要
以甘草酸为原料,以杂多酸作为催化剂,采用水热法合成了乙酰甘草次酸甲酯;采用元素分析、薄层层析、质谱和红外光谱等方法表征了所合成的产物。
Methyl Glycyrrhetate Acetate was synthesized successfully by hydrothermal method with Glycyrrhizic Acid while using Heteropoly Acid as catalyst.The samples were characterized by the element analysis,thin layer chromatography(TLC),fourier transform infrared(FT-IR) and Mass Spectroscopy(MS) techniques et al.
出处
《吉林农业大学学报》
CAS
CSCD
北大核心
2008年第3期297-300,共4页
Journal of Jilin Agricultural University
基金
吉林省科技发展计划项目(20011109)
关键词
甘草酸
水热法
乙酰甘草次酸甲酯
合成
杂多酸
glycyrrhizic acid hydrothermal method methyl glycyrrhetate acetate synthesis heteropoly acid