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气相色谱法测定角鲨烯软胶囊中角鲨烯含量 被引量:10

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摘要 目的 建立角鲨烯软胶囊中角鲨烯的气相色谱测定方法。方法 采用气相色谱内标法,FID检测器,硅酮OV-17填充柱(2m×3.2mm),柱温250℃,进样口温度280℃,监测器温度300℃。结果 角鲨烯在1.2-19.2μg内呈良好的线性关系,加样回收率为99.8%。结论 该方法简单可靠,精度高,适用于角鲨烯软胶囊中角鲨烯的含量测定。
作者 车欣颖 卢雯
出处 《齐齐哈尔医学院学报》 2008年第12期1475-1476,共2页 Journal of Qiqihar Medical University
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