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制备1-氰基-2,3,5-三-O-苯甲酰基-β-D-呋喃核糖的简便方法 被引量:3

Synthesis of 1 Cyano 2,3,5 tri O benzoyl β D ribofuranose
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摘要 制备1┐氰基┐2,3,5┐三┐O┐苯甲酰基┐β┐D┐呋喃核糖的简便方法张万轩*雷策南黄锦霞陈家威(湖北大学化学系武汉430062)关键词鸟苷,制备,氰基三苯甲酰基-β-D-呋喃核糖,三甲基氯硅烷1996-08-12收稿,1997-03-05修回1-氰... Reacting guanosine with benzoyl chloride gave a mixture containing 2,3,5 tribenzoyl guanosine. After distillation in vacuum the residual solid was acetylated directly and 1 O acetyl 2,3,5 tri O benzoyl β D ribofuranose (2) was obtained. Being reacted with Me 3SiCN, (2) led to the title compound(1). The method reported here is more convenient and cheaper with a considerably higher yield.
机构地区 湖北大学化学系
出处 《应用化学》 CAS CSCD 北大核心 1997年第3期115-116,共2页 Chinese Journal of Applied Chemistry
关键词 鸟苷 氰基 三苯甲酰基 呋喃核糖 核糖 核苷 guanosine,cyano tri O benzoyl β D ribofuranose,synthesis,chloro trimethylsilane
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