摘要
制备1┐氰基┐2,3,5┐三┐O┐苯甲酰基┐β┐D┐呋喃核糖的简便方法张万轩*雷策南黄锦霞陈家威(湖北大学化学系武汉430062)关键词鸟苷,制备,氰基三苯甲酰基-β-D-呋喃核糖,三甲基氯硅烷1996-08-12收稿,1997-03-05修回1-氰...
Reacting guanosine with benzoyl chloride gave a mixture containing 2,3,5 tribenzoyl guanosine. After distillation in vacuum the residual solid was acetylated directly and 1 O acetyl 2,3,5 tri O benzoyl β D ribofuranose (2) was obtained. Being reacted with Me 3SiCN, (2) led to the title compound(1). The method reported here is more convenient and cheaper with a considerably higher yield.
出处
《应用化学》
CAS
CSCD
北大核心
1997年第3期115-116,共2页
Chinese Journal of Applied Chemistry
关键词
鸟苷
氰基
三苯甲酰基
呋喃核糖
核糖
核苷
guanosine,cyano tri O benzoyl β D ribofuranose,synthesis,chloro trimethylsilane