期刊文献+

HPLC法测定卫矛醇及检测复方中药制剂通痹灵中的卫矛醇 被引量:9

Determination of Dulcitol in Traditional Chinese Compound Priscription "Tongbilin" by HPLC
下载PDF
导出
摘要 用HPLC测定复方中药制剂通痹灵中的卫矛醇。以衍生物制备法将卫矛醇和内标制成具有紫外吸收的异氰酸苯酯衍生物,用TSK-gelODS-80TM柱,乙腈-乙醇-水(5:2:3)为流动相,检测波长240mm,内标法定量。 Dulcitol in traditional Chinese compound prescription 'Tongbilin' was determined by HPLC. This method is based on the fact that polyols like dulcitol and glucose diethyl mercaptol (internal standard) can react with phenylisocyanate to yield UV-absorbing derivatives which can be detected at 240 nm by HPLC. A TSK-gel ODS-80TM column and mobile phase acetonitrile-ethanol-H2O(5: 2: 3) were employed
出处 《中草药》 CAS CSCD 北大核心 1997年第12期718-721,共4页 Chinese Traditional and Herbal Drugs
  • 相关文献

参考文献7

共引文献17

同被引文献108

引证文献9

二级引证文献42

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部