摘要
用微波辐射法合成了介孔分子筛MCM-41,采用浸渍法获得不同钯含量的Pd-MCM-41催化剂,用XRD、低温N2吸附-脱附、IR对MCM-41及组装体进行了表征;研究了Pd负载量、反应时间、反应温度等条件对葡萄糖氧化反应的影响,结果表明Pd-MCM-41能有效催化葡萄糖氧化反应。
Mesoporous molecular sieve MCM-41 was synthesized by microwave radiation method. Pd- MCM-41 with different Pd content were prepared from MCM-41 and PdCl2 by impregnation method. The MCM-41 and Pd-MCM-41 were characterized by XRD, low temperature N2 dsorption/desorption and IR. The catalytic performance of Pd-MCM-41 for oxidation of glucose was studied.
出处
《化学世界》
CAS
CSCD
北大核心
2008年第11期641-643,666,共4页
Chemical World