摘要
目的:用HPLC法测定鼻康宝胶囊中黄芩苷的含量。方法:采用Kromasil C18柱,以甲醇-水-磷酸(40:60:0.2)为流动相,检测波长280nm。结果:黄芩苷在5.2~83.2μg/mL范围内峰面积与浓度呈良好性线形关系,r=0.9998,平均回收率为97.8%。结论:该方法专属性强、简便、精密度好、结果准确可靠。
Objective: To establish a method for determination of baiealin in Bikangbao capsule by HPLC. Methods: HPLC was performed on Kromasil C18 column with methanol-water- phosphonic acid (40: 60: 0.2) as mobile phase. The UV detection wavelength was 280 nm. Results: The linear range of baicalin was sample size 5.2 - 83.2 μg/mL ( r = 0. 9998 ) , the average recovery was 97.8%. Conclusions : The method was simple, accurate and fast, and could be used for the determination of baicalin in Bikangbao capsule.
出处
《儿科药学杂志》
CAS
2009年第1期43-44,共2页
Journal of Pediatric Pharmacy
关键词
鼻康宝胶囊
黄芩苷
高效液相色谱法
Bikangbao capsule
Baicalin
High performance liquid chromatography