期刊文献+

光果莸不同器官挥发油化学成分分析 被引量:2

Analysis of Essential Oil from Different Organs of Caryopteris tangutica
原文传递
导出
摘要 目的:分析研究光果莸挥发油的主要化学成分。方法:采用共水蒸馏法分别提取光果莸茎、叶和花的挥发油,应用气相色谱-质谱联用(GC-MS)技术并结合Kovats保留指数(K I)对比法对挥发油化学成分进行了鉴定,运用面积归一化法确定了各组分的相对含量。结果:从茎、叶及花中分别鉴定出13、48和42种成分。其中花和叶中的主要成分及相对含量均相似,分别为桃金娘烯醛(2.73%,1.69%)、反-乙酸松香芹酯(46.69%,55.48%)、乙酸桃金娘烯酯(1.17%,1.42%)、β-柏木烯(1.62%,3.21%)及石竹烯氧化物(1.67%,2.73%)等。茎中的化学成分与花和叶中化学成分的相差较大,主要成分为反-乙酸松香芹酯(24.19%)、棕榈酸(47.32%)和植醇(0.77%)等。结论:光果莸茎、叶及花的挥发油均含有大量的活性成分,具有较高的应用潜力和综合开发前景。 Objective: To study the main chemical components of essential oils from Caryopteris tangutica. Methods: The chemical compositions of essential oils obtained by hydrodistillation from different organs of Caryopteris tangutica were separately analyzed and i- dentified by GC-MS and Kovats retention index. The relative contents of the components by the peak-area normalization method adopted in gas chromatography. Results: 13,48 and 42 components were separately identified from stems, leaves and flowers. The components and relative contents of the leaves were similar with the flowers, and the main constituents were Myrtenal( 2. 73%, t. 69% ), trans-Pinoearvyl acetate(46. 69% ,55.48% ), Myrtenyl acetate ( 1.17%, 1.42% ) ,β-Cedrene ( 1.62%, 3.21% ), Caryophyllene oxide ( 1.67%, 2.73%)and so on. The components of the stems were different from others, and the main constituents were hexadecanoie acid (47. 32% ) ,trans-Pinocarvyl acetate(24. 19% ) ,phytol(0. 77% ). Conclusion:The components and relative contents of the essential oils among stems,leaves and flowers were distinctly different,and each of them had a great range of potential utilities and a prospect of development.
作者 闫平 王喆之
出处 《中药材》 CAS CSCD 北大核心 2009年第1期61-65,共5页 Journal of Chinese Medicinal Materials
基金 陕西省科学技术研究发展计划项目(2005K16-G9)
关键词 光果莸 挥发油 Kovats保留指数 气相色谱-质谱 Caryopteris tangutica Maxim. Essential oil KI GC-MS
  • 相关文献

参考文献8

  • 1西北植物研究所.秦岭植物志[M].北京:科学出版社,1983.
  • 2杨爱梅,鲁润华,柳军玺,史高峰.光果莸挥发油成分研究[J].中国中药杂志,2005,30(3):233-234. 被引量:5
  • 3ADAMS R P. Identification of essential oil components by gas chromatography/quadrupole mass Spectroscopy [M]. Carol Stream, Illinois. USA : Allured Publishing Corporation ,2001 : 1-40.
  • 4钟瑞敏,曾庆孝,张振明,王羽梅,彭华贵.气质联用结合保留指数对比在五种木兰科芳香精油成分鉴定中的应用[J].分析测试学报,2006,25(5):16-20. 被引量:32
  • 5ISIDOROV V A, KRAJEWSKA U, V INOGOROVA V T, et al. Gas chromatographic analysis of essential oil from buds of different birch specieswith preliminary partition of compounents[J]. Biochemical Systematics and Ecology, 2004,32 : 1-13.
  • 6KOVATS E. Gas chromatographic characterization of organic substances in the retention index system [ J ]. Adv ChRom atogr, 1965, ( 1 ) :229-247.
  • 7VAN D, DOOL H, KRATZ PD. A generalization of retention indexsystem including linear temperature programmed gas-liquid partition chromatography [ J ]. J Cherom atogr , 1963,11:463-471.
  • 8MARY ANNE S. LIMA, EDtLBERTO R. SIL VEIRA, et al. Biologically Active Flavonoids and Terpenoids from Egletes viscosa[J]. Phytochemistry, 1996,41 ( 1 ) :217-223.

二级参考文献9

  • 1刘玉壶.木兰科分类系统的初步研究[J].植物分类学报,1984,22(2):89-109.
  • 2陈永宝.微生物学实验与指导[M].北京:中国医药科技出版社,1994.142.
  • 3Adams R P. Identification of essential oils by ion trap mass spectroscopy. New York: Academic Press, 1989.
  • 4丛蒲珠.质谱在天然有机化学中的应用[M].北京:科学出版社,1987..
  • 5El-MASSRY K F,El-GHORAB A H,FAROUK A.Antioxidant activity and volatile components of Egyptian Artemisia judaica L[J].Food Chemistry,2002,79:331-336
  • 6ADAMS R P.Identification of essential oil components by gas chromatography/quadrupole mass spectroscopy[M].Carol Stream,Illinois.USA:Allured Publishing Corporation,2001:1-40.
  • 7ISIDOROV V A,KRAJEWSKA U,VINOGOROVA V T,et al.Gas chromatographic analysis of essential oil from buds of different birch species with preliminary partition of components[J].Biochemical Systematics and Ecology,2004,32:1 -13.
  • 8徐凤霞,陈忠毅,张奠湘.木兰科的分支分析[J].热带亚热带植物学报,2000,8(3):207-214. 被引量:16
  • 9张永红,汪汉卿,郭新华,芦志刚.光果莸的化学成分研究[J].中草药,2001,32(12):1069-1070. 被引量:3

共引文献37

同被引文献21

  • 1杨爱梅,鲁润华,柳军玺,史高峰.光果莸挥发油成分研究[J].中国中药杂志,2005,30(3):233-234. 被引量:5
  • 2中国科学院中国植物志编辑委员会.中国植物志(第六十五卷第一册)[M].北京:科学出版社,1999:202.
  • 3西藏昌都医算学院.晶镜本草本草[M].北京:中央民族出版社,1995:270.
  • 4SLAVICA G,DZAMIC M,MIHAILO S,et al.Essential oil composition of stachys anisochila[J].Chemistry of Natural Compounds,2011,47(5):823-825.
  • 5SLAVKOVSKA V,COULADIS M,BOJOVIC S,et al.Essential oil and its systematic significance in species of Micromeria Bentham from Serbia&Montenegro[J].Plant Systematics and Evolution,2005,10(255):1-15.
  • 6COLE R A,BANSAL A,MORIARITY D M,et al.Chemical composition and cytotoxic activity of the leaf essential oil of Eugenia zuchowskiae from Monteverde[J].Costa Rica J Nat Med,2007,61:414-417.
  • 7HU H B,ZHENG X D,HU H S,et al.Chemical compositions and Anti-microbial activities of essential oils extracted from Acanthopanax brachypus[J].Archives of Pharmacal Research,2009,32(5):699-710.
  • 8NADHIR G,MOHAMED Y,ISABELLE B,et al.Seasonal variation of chemical composition and antioxidant activity of essential oil from Pistacia atlantica Desf.leaves[J].J Am Oil Chem Soc,2010,87:157-166.
  • 9王萍,张银波,江木兰.多不饱和脂肪酸的研究进展[J].中国油脂,2008,33(12):42-46. 被引量:255
  • 10周永红,王延,宋湛谦.α-蒎烯合成杀虫增效剂的研究[J].林产化学与工业,1998,18(1):1-11. 被引量:31

引证文献2

二级引证文献2

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部