A Novel Approach for Determining the Orientation of 3-Hydroxyl Group of Some Steroids by CIMS

A Novel Approach for Determining the Orientation of 3-Hydroxyl Group of Some Steroids by CIMS

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摘要 Trimethylchlorosilane was used as a stereoselective reagent to determine the e or a orientation of 3-hydroxyl group of some steroids by chemical ionization mass spectrometry. Trimethylchlorosilane was used as a stereoselective reagent to determine the e or a orientation of 3-hydroxyl group of some steroids by chemical ionization mass spectrometry.

作者 Yuan Jiang PAN Yao Zu CHEN(Department of Chemistry, Zhejiang University, Hangzhou 310027)

出处《Chinese Chemical Letters》 SCIE CAS CSCD 1999年第2期143-144,共2页 中国化学快报（英文版）

关键词 orientation of 3-hydroxyl group STEROIDS mass spectrometric determination orientation of 3-hydroxyl group steroids mass spectrometric determination

分类号 O629 [理学—有机化学]

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1李文华,王锦华,胡振元.STUDIES ON FLUORO-ALKYL BONDED PHASE AS HPLC PACKING[J].Chinese Science Bulletin,1982,27(5):574-575.
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3季小慎,王雪峰.9-羧基氧杂蒽类化合物的合成及质谱裂解规律[J].质谱学报,1998,19(2):54-56.
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Chinese Chemical Letters

1999年第2期

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A Novel Approach for Determining the Orientation of 3-Hydroxyl Group of Some Steroids by CIMS

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