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火焰原子吸收光谱法测定奶粉中金属元素 被引量:10

FAAS Determination of Metal Elements in Milk Powder
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摘要 采用灰化酸溶法处理样品,火焰原子吸收光谱法测定婴幼儿奶粉中钾、钙、钠、锌、铁和镁6种金属元素的含量。对仪器的工作条件作了详细的叙述。吸光度与6种金属元素的质量浓度之间均呈线性关系。应用此法测得3种婴幼儿奶粉中上述6元素的含量分别为779.41,563.69,779.37 mg/100 g(钾),627.56,430.33,488.6 mg/100 g(钙),254.6,163.5,223.3 mg/100 g(钠),5.90,4.98,6.04 mg/100 g(锌),8.86,7.11,8.00 mg/100 g(铁),55.2,46.4,81.3 mg/100 g(镁)。以上数值均符合国家标准(GB 10766-1997)的规定。 Amounts of K, Ca, Na, Zn, Fe and Mg in 3 brands of infant milk powder were determined by flame atomic absorption spetrometry. The samples were treated by ashing and acid dissolution. The working conditions of the instrument were described in detail. Linear relationships between values of absorbances and mass concentrations of the 6 metal elements were obtained. Concents obtained were 779. 41, 563. 69, 779. 37 mg/100 g (K), 627.56, 430. 33, 488. 6 rag/100 g (Ca), 254.6, 163. 5, 223. 3 mg/100 g (Na), 5. 90, 4.98, 6. 04 mg/100 g (Zn), 8. 86, 7. 11, 8. 00 mg/100 g (Fe) and 55. 2, 46. 4, 81. 3 mg/100 g (Mg), respectively. The values mentioned above were in agreement with the requirements of national standard GB/T 10766-1997.
出处 《理化检验(化学分册)》 CAS CSCD 北大核心 2009年第5期512-513,共2页 Physical Testing and Chemical Analysis(Part B:Chemical Analysis)
关键词 火焰原子吸收光谱法 灰化酸溶法 金属元素 奶粉 Flame atomic absorption spectrometry Ashing and acid dissolution method Metal elements Milk powder
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  • 1颜世铭.微量元素导论[M].上海:同济大学出版社,1997.
  • 2Ikem A, Nwankwoala A, Odueyungbo S, et al. Level of 26 elements in infant formula from USA, UK, and Nigeria by microwave digestion and ICP-OES[J]. Food Chem, 2002, 77:39-447.
  • 3Baker SS, Cochran WJ, Flores CA, et al. Iron fortficationofinfant formulas[J]. Pediatrics, 1999,104 : 119-123.
  • 4Glade MJ. Conference review. Third international symposium on the role of soy in preventing and treating chronic disease,Washington, DC. October 31-November 1[R]. Nutrition,2001,17:73-77.
  • 5Hua KM, Kay M, Indyk HE. Nutritional element analysis in infant formulas by direct dispersion and inductively coupled plasma-optical emission spectrometry[J]. Food Chem, 2000,68:463-470.
  • 6Rodriguez Rodriguez EM, Sanz Alaejos M, Diaz Romero C.Concent tions of iron, copper and zinc in human milk and powdered infant formula[J]. Int J Food Sci Nutr, 2000,51:373-380.
  • 7苏志刚,曹云娣,乔建华,方家琪.原子吸收法测定磷矿和肥料中的钙和镁[J]光谱学与光谱分析,1987(04).
  • 8黄伟坤.食品检验与分析[M]中国轻工业出版社,1993.
  • 9原子吸收光谱分析编写组.原子吸收光谱分析[M]地质出版社,1979.
  • 10刘宇,刘立行,于智明,范佩霞.乳化法-火焰原子吸收光谱法测定奶粉中的锌[J].分析试验室,1997,16(4):60-63. 被引量:9

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