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高效液相色谱法测定安痛藤中羽扇豆醇的含量 被引量:3

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摘要 目的建立安痛藤中羽扇豆醇含量的测定方法。方法采用高效液相色谱(HPLC)法,色谱柱为diamonsil C18(5μm,250 mm×4.6 mm),流动相为甲醇∶水=98∶2,流速1.0 ml.min-1,检测波长206 nm,柱温为30℃。结果羽扇豆醇在0.316~3.16μg范围内与峰面积有良好线性关系,r=0.999 5,平均回收率为97.82%,RSD为2.49%。结论该方法测定安痛藤中羽扇豆醇含量快速、简便、准确、可靠。
出处 《时珍国医国药》 CAS CSCD 北大核心 2009年第5期1086-1087,共2页 Lishizhen Medicine and Materia Medica Research
基金 2006年江西省教育厅科技项目(No.[2006]226号)
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