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多杀菌素的高效液相色谱测定 被引量:17

Determination of Spinosad with High-Performance Liquid Chromatography
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摘要 本文建立了高效液相色谱法测定多杀菌素的定量分析方法,本方法的相对标准偏差为1.3441,变异系数为1.8067%,线性相关系数为0.99959,平均回收率达到99.2429%,最后采用液质联用方法对目标化合物进行验证。 A quantitative analytical method was established for spinosad content determination with HPLC. Results showed that the standard deviation, coefficient of variation, linear correlation, and average recovery were 1.3441, 0.99959, 0.99959, and 99.2429%, respectively. The target compound was also validated with LC-MS.
出处 《现代食品科技》 EI CAS 2009年第6期704-706,共3页 Modern Food Science and Technology
基金 国家科研院所社会公益研究专项(2005DIB4J151) 国家自然科学基金(20436020、50573025)
关键词 多杀菌素 高效液相色谱法 液质联用 spinosad HPLC LC-MS
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