摘要
以六氢哒嗪为先导化合物,合成了13个新型六氢哒嗪衍生物,通过IR,1HNMR和MS进行了结构表征,对其中3个代表性的化合物培养了单晶,获得了X射线衍射结构.初步的生测结果表明部分化合物具有除草活性.
Thirteen novel hexahydropyridazine derivatives were synthesized based on hexahydropyridaz- ine. And structurally confirmed by IR, 1H NMR and mass spectra. The crystal structures of la, 2a and 3a were determined by X-ray diffraction analysis. Preliminary bioassays show that some of the compounds have herbicidal activities.
出处
《有机化学》
SCIE
CAS
CSCD
北大核心
2009年第8期1232-1235,共4页
Chinese Journal of Organic Chemistry
基金
浙江省应用化学重中之重学科开放课题资助项目
关键词
六氢哒嗪
氨基甲酰基六氢哒嗪
三唑并哒嗪
合成
除草活性
hexahydropyridazine
hexahydropyridazine-l-carboxamide
1,2,4-triazolo[1,2-a]pyridazine
synthesis
herbicidal activity
