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Syntheses and Crystal Structures of One-dimensional Ni(Ⅱ) Complexes with 5-Tert-butyl Isophthalic Acid 被引量:1

Syntheses and Crystal Structures of One-dimensional Ni(Ⅱ) Complexes with 5-Tert-butyl Isophthalic Acid
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摘要 Two new Ni( Ⅱ) coordination polymers, {[Ni(tbip)(bipy)(H2O)]-0.5H2O}n 1 and [Ni(tbip)(phen)(H2O)]n 2 (Hatbip = 5-tert-butyl isophthalic acid, bipy = 2,2'-bipyridine, phen = 1,10-phenanthroline), have been synthesized under hydrothermal conditions and characterized by elemental analysis, X-ray diffraction, and IR spectroscopy. In the two polymers, H2tbip acts as a tridentate ligand. Compound 1 has a tbip bridged 1-D linear chain which is extended by hydrogen bonds into a 1-D double chain, while compound 2 exhibits a 1-D zigzag chain. Two new Ni( Ⅱ) coordination polymers, {[Ni(tbip)(bipy)(H2O)]-0.5H2O}n 1 and [Ni(tbip)(phen)(H2O)]n 2 (Hatbip = 5-tert-butyl isophthalic acid, bipy = 2,2'-bipyridine, phen = 1,10-phenanthroline), have been synthesized under hydrothermal conditions and characterized by elemental analysis, X-ray diffraction, and IR spectroscopy. In the two polymers, H2tbip acts as a tridentate ligand. Compound 1 has a tbip bridged 1-D linear chain which is extended by hydrogen bonds into a 1-D double chain, while compound 2 exhibits a 1-D zigzag chain.
出处 《Chinese Journal of Structural Chemistry》 SCIE CAS CSCD 2009年第9期1061-1066,共6页 结构化学(英文)
基金 supported by the National Natural Science Foundation of China (Nos.20771026 and 20771054) the Henan Tackle Key Problem of Science and Technology (Nos.072102270030 and 072102270034) the Foundation of Education Committee of Henan Province (2006150017 and 2008A150018)
关键词 Ni(Ⅱ) complex 5-tert-butyl isophthalic acid crystal structure Ni(Ⅱ) complex, 5-tert-butyl isophthalic acid, crystal structure
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