摘要
The synthesis of a new Schiff base(salicylaldehyde-fluorenylamine) with fluorene was reported.The molecular structure was characterized by IR,1H NMR,MS and elementary analysis.The crystal structure was determined by X-ray diffraction method.The crystal belongs to monoclinic,space group P2(1)/c with a =1.60170(6)nm,b=0.82261(8)nm,c=1.11693(2)nm,β=96.671(7)°,V= 1.4617(2) nm3,Z=4,Dc = 1.297g/cm3,μ(MoKα) = 0.080mm-1,F(000) = 600,R1= 0.0857,WR2= 0.1989.The biological activity test indicated that it was an effective bactericide on bacillus such as Staphylococcus aureus,Bacillus thuring Iensis and Bacillus subtilis.
The synthesis of a new Schiff base（salicylaldehyde-fluorenylamine） with fluorene was reported.The molecular structure was characterized by IR,1H NMR,MS and elementary analysis.The crystal structure was determined by X-ray diffraction method.The crystal belongs to monoclinic,space group P2（1）/c with a =1.60170（6）nm,b=0.82261（8）nm,c=1.11693（2）nm,β=96.671（7）°,V= 1.4617（2） nm^3,Z=4,Dc= 1.297g/cm^3,μ（MoKα） = 0.080mm^-1,F（000） = 600,R1 = 0.0857,WR2 =0. 1989. The biological activity test indicated that it was an effective bactericide on bacillus such as Staphylococcus aureus, Bacillus thuring lensis and Bacillus subtilis.
出处
《化学研究与应用》
CAS
CSCD
北大核心
2009年第11期1571-1574,共4页
Chemical Research and Application
基金
黄石理工学院科研项目(08yjz27B)资助
关键词
水杨醛
2-芴胺
席夫碱
晶体结构
生物活性
salicylaldehyde
2-fluoreylamine
Schiff base
crystal structure
biological activity
