摘要
以金黄色葡萄球菌为工作菌, 用杯碟法测定氧氟沙星(OFL)在畜禽粪便中的残留。结果表明:鸡粪便中氧氟沙星的最低检测限为0.156μg/g,标准曲线的工作范围为0.156~5.00μg/g,工作曲线的日内变异系数在2.4%~3.3%、日间变异系数为3.7%~5.2%,回收率分别为79.49%~87.92%。因此,建立的方法可以满足鸡粪尿混合物中氧氟沙星的残留检测要求。
Ofloxacin residues in faeces of chicken were determined using cylinder plate method, taking Micro- coccus luteus 26003 as the test microorganism. Results showed that the detection limit of ofloxacin in faeces was 0.156 Ixg/g, and the calibration curve was linear within the range of 0.156-5.00 μg/g, variation for the microbiological method were 2.4%-3.3% in intra-assay and 3.7%-5.2% recoveries in faeces of chicken ranged from 79.49% to 87.92%.
出处
《中国农学通报》
CSCD
北大核心
2009年第23期31-33,共3页
Chinese Agricultural Science Bulletin
基金
国家科技富民强县专项行动计划:(铜陵县)渔牧结合高效循环养殖技术集成示范与推广
现代农业(蛋鸡)产业技术体系建设专项资金
公益性行业蛋鸡科研专项"优质土鸡蛋生产关键技术研究与示范"(NYHYZX07-039)
关键词
氧氟沙星
粪便
微生物法
残留
标准曲线
ofloxacin, faeces, microbiological method, residues, calibration curve