摘要
对氯亚磷结构进行修饰,连接一个六碳的间隔臂,制得亚胺硫磷、氯亚磷的半抗原,确定最佳反应条件。利用薄层层析和质谱法,对反应进行实时监控,确定最佳反应时间为16d。通过EDC法成功制备亚胺硫磷和氯亚磷人工抗原。
The phosmet structure was modified, interval arm of six-carbon were linked, and the hapten compound of dialifor and phosmet were prepared and meanwhile the optimum reaction time were determined in this paper. The reaction was real-time monitor by TLC and MC. The results showed that the best reaction time was 16 days. And dialifor and posemet artificial antigen were successfully prepared with ECD method.
出处
《农产品加工（下）》
2009年第12期4-6,共3页
Farm Products Processing
基金
国家"863"计划课题项目(2006AA10Z448)
天津科技大学引进人才基金项目(20080402)
