期刊文献+

多级定转子连续分散混合器内的微观混合性能 被引量:3

Micromixing characteristics in a continuous rotor-stator mixer
下载PDF
导出
摘要 采用碘化物-碘酸盐平行竞争反应作为工作体系,对多级定转子连续分散混合器内(CRS)的微观混合特性进行了实验研究,得到了流量、转速、浓度、体积比等因素对离集指数的影响规律。结果表明该体系对H^+浓度比较敏感,在转速为3000~6800r/min范围内,离集指数随转速增加而下降;在低操作转速下,随着流量增加,离集指数先迅速减小后缓慢增加。与常见的搅拌反应器相比,多级定转子连续分散混合器具有优良的微观混合性能,特别适合于快速反应过程。 The micromixing characteristics in a continuous rotor-stator mixer (CRS) have been studied experimentally by using the iodide-iodate parallel competing reactions system. The influence of flow rate, rotor speed, concentration and volume ratio on the segregation index (Xs) has been investigated. The experimental results show that the reaction system is sensitive to H ^+ concentration. The segregation index decreases with the increase of rotor speed in the range 3000 to 6800 r/min. When the rotor speed is low, the segregation index decreases sharply at first, and then increases more slowly as the flow rate increases. The CRS mixer has a better micromixing performance than commonly used stirred reactors and is especially suitable for fast reaction systems.
出处 《北京化工大学学报(自然科学版)》 CAS CSCD 北大核心 2010年第1期1-4,共4页 Journal of Beijing University of Chemical Technology(Natural Science Edition)
基金 国家自然科学基金(20821004)
关键词 连续分散混合器 微观混合 碘化物-碘酸盐反应体系 离集指数 CRS micromixing iodide-iodate reaction system segregation index
  • 相关文献

参考文献8

  • 1刘骥,陈建峰,宋云华,郑冲.旋转填充床中微观混合实验研究[J].化学反应工程与工艺,1999,15(3):327-332. 被引量:19
  • 2Barailler F, Heniche M, Tanguy P A. CFD Analysis of a rotor-stator mixer with viscous fluids[ J]. Chemical Engineering Science, 2006, 61 (9): 2888- 2894.
  • 3Bourne J R, Garcia-Rosas J. Rotor-stator mixers for rapid micromixing[J]. Chem Eng Res Des, 1986, 64(1): 11 - 17.
  • 4Chu G W, Song Y H, Yang H J, et al. Mieromixing efficiency of a novel rotor-stator reactor[ J]. Chemical Engineering Journal, 2007, 128(2/3) :191 -196.
  • 5张占元,闵健,高正明.连续高速分散混合器内的微观混合性能[J].北京化工大学学报(自然科学版),2008,35(5):4-7. 被引量:3
  • 6Fournier M C, Falk L, Villermaux J. A new parallel competing reaction system for assessing micromixing effi- ciency-experimental approach[ J]. Chemical Engineering Science, 1996, 51 (22) : 5053 -5064.
  • 7Guichardon P, Falk L. Characterization of micromixing efficiency by the iodide-iodate reaction system. Part Ⅰ: Experimental procedure [ J]. Chemical Engineering Science, 2000, 55(19): 4233-4243.
  • 8Guichardon P, Falk L, Villermaux J. Characterisation of micromixing efficiency by the iodide-iodate reaction system. Part Ⅱ: Kinetic study [ J]. Chemical Engineering Science, 2000,55 ( 19 ) :4245 - 4253.

二级参考文献16

  • 1Lin W W,Chem Eng Sci,1997年,52卷,21/22期,3837页
  • 2郭锴,学位论文,1996年
  • 3陈建峰,搅拌反应釜中微观混合问题,1989年
  • 4天津大学物理化学教研室,物理化学.下(第2版),1983年,173页
  • 5Bourne J R. Mixing and the selectivity of chemical reactions[J]. Org Process Research Development, 2003, 7 (4): 471 - 508.
  • 6Barailler F, Heniche M, Tanguy P A. CFD Analysis of a rotor-stator mixer with viscous fluids[J]. Chemical Engi- neering Science, 2006, 61(9):2888 - 2894.
  • 7Bolzern O, Bourne J R. Rapid chemical reactions in a centrifugal pump[J]. Chemical Engineering Research & Design, 1985, 63 : 275 - 282.
  • 8Bourne J R, Garcia-Rosas J. Rotor stator mixers for rapidmicromixing[J]. Chemical Engineering Research & Design, 1986,64: 11-17.
  • 9Padron G A. Measurement and comparison of power draw in batch rotor-stator mixer[ D]. Maryland: University of Maryland, 2001.
  • 10Fournier M C, Falk L, Villermaux J. A new parallel competing reaction system for assessing mieromixing efficiency-experimental approaeh[J ]. Chemical Engineering Science, 1996, 51(22) : 5053 - 5064.

共引文献20

同被引文献28

引证文献3

二级引证文献10

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部