摘要
目的:探讨蟾皮经水烫炮制后脂蟾毒配基含量变化。方法:采用高效液相法测定。结果:3批蟾皮中脂蟾毒配基含量依次为(mg/g):06253,06102,06433;对应3批水烫炮制品含量为(mg/g):07864,07716,07986。平均回收率9834%,RSD=128%。结论:蟾皮水烫炮制品较生品中脂蟾毒配基含量略高。
Objective:To investigate the effect of scald processing on the content of recibufogenin in Pellis Sicci Bufonis.Method:Samples were analyzed by high performance liquid chromatography.Result:The content of recibufogenin in the scald processed product was 25.7% higher than that in the unprocessed one.The average recovery was 98.34% and RSD 1.28%.Conclusion:The results indicate that the content of recibufogenin in scald processed Pellis Sicci Bufonis is higher than that in the unprocessed drug.
出处
《中国中药杂志》
CAS
CSCD
北大核心
1998年第9期533-534,共2页
China Journal of Chinese Materia Medica