摘要
以对苯二甲醛为原料,制得对苯基双异硫氰酸酯,再和L构型的氨基酸反应制得11种含有双杂环基团的对苯基双乙内酰硫脲类衍生物,其中有9种未见文献报道。产物经1HNMR、13CNMR和元素分析得到了确认和表征。
Eleven p-phenyl-bis-thiohydantoins derivatives containing two heterocyelic structures were synthesized from L-amino acid and p-phenylene diisothiocyanate, which was obtained from p-phenyl-dimethanal. Among these products nine of them have not been reported previously. The title compounds reported were characterized by means of IHNMR,1SCNMR and elemental analysis.
出处
《化学试剂》
CAS
CSCD
北大核心
2010年第2期114-116,共3页
Chemical Reagents
基金
河南省自然科学基金资助项目(0611021700)
河南省教育厅自然科学基金资助项目(2007150024)
