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不同产地何首乌药材水分、灰分和浸出物的测定 被引量:8

Determination of water,ash,and extract in Polygonum multiflorum form different sources by HPLC
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摘要 目的:测定何首乌药材的水分、灰分和浸出物的含量,为何首乌药材质量标准的修订提供实验数据。方法:按《中国药典》2005年版一部附录ⅨH中水分测定法中的第一法、附录ⅨK灰分测定法和附录ⅩA浸出物测定法测定。结果:何首乌药材含水量均不超过10.77%,总灰分不高于6.04%,酸不溶性灰分不高于0.71%,冷浸法醇溶性浸出物含量不低于20.03%。结论:本方法为何首乌药材质量标准的修订提供了实验数据。 Objective: To determine the fleece-flower root herbs moisture, ash, and extract the examination can provide experimental data for the revised quality standards in Polygonum multiflorum. Methods: According to Chinese Pharmacopoeia in 2005 edition of an appendix IX H determination of water in the first method, appendix IX K ash assay and Appendix X A extract determination method to determinate the content. Results: The fleece-flower root water content of no more than 10.77% herbs, no more than 6.04% total ash, acid insoluble ash not more than 0.71%, alcohol-soluble extract of the cold soak method the amount of not less than 20.03%. Conclusion: Revised Standard of fleece-flower root herbs can provide the experimental data.
出处 《中国医药导报》 CAS 2010年第13期61-62,共2页 China Medical Herald
关键词 何首乌 水分测定 灰分测定 浸出物测定 Polygonum multiflorum Moisture determination Ash determination Extract determination
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