摘要
目的建立解痹胶囊的质量标准。方法采用HPLC法对解痹胶囊中士的宁的含量进行测定。结果解痹胶囊中士的宁的含量在0.7488—5.6160μg的范围内,有良好的线性关系,r=0.9999,平均回收率为100.55%,RSD为1.44%。结论建立了解痹胶囊的质量标准,该方法操作易行,稳定可靠,用于解痹胶囊中士的宁的含量,可以用于该制剂的质量控制。
Objective: To establish a standard for determination of Strychnine in Jiebi capsules. Method: Strychnine in Jiebi capsules by HPLC. Result: The linear range of Strychnine was 0.7488-5.6160 μg , r=0.9999. The average recovery of Strychnine was 100.55%and RSD was 1.44%. Conclusion: The method is simple ,sensitive and aeeurte and can be used to determine Strychnine in Jiebi capsules and quality control of Jiebi Capsules.